CHEM 322L SYLLABUS Dr. DiLella
INSTRUMENTAL ANALYSIS LAB Spring 2008
DESCRIPTION
CHEM 322L is a one-credit laboratory course that provides hands-on experience using
modern analytical instrumentation and techniques. Students learn how to prepare samples for
and how to operate several types of instruments. Topics covered include atomic spectroscopy,
molecular spectroscopy, electrochemistry, mass spectroscopy and chromatography.
Students are introduced to and are expected to use advanced data handling and error
treatment methods. Personal computers are available for use in data analyses. Students are
expected to use a computer spreadsheet program for data analysis and presentation.
TEXT
Lab Manual is available in the bookstore
OFFICE HOURS
MWF 10-11, 3-4 R 1-2 or by appointment
Byrd Center 113 304-876-5430 ddilella@shepherd.edu
web page: http://WEBPAGES.SHEPHERD.EDU/DDILELLA/
CLASS HOURS
R 2:10 - 5:00
PREREQUISITES
CHEM 209, 209L are required. CHEM 321 and CHEM 321L are strongly recommended.
CHEM 322 should be taken concurrently
Computer skills are not a prerequisite but students who do not know how to do basic
computer spreadsheet operations should see the instructor as soon as possible to get special
tutoring in these skills. With the aid of a computer spreadsheet program, the time required to
do the lab reports will be significantly reduced.
SAFETY
The experiments have been designed with safety as a major consideration. If everything
went as planned there would be little danger. However, the equipment and procedures will be
unfamiliar and mistakes can and will occur. Be sure that you understand the hazards associated
with the equipment before starting an experiment. Do not be afraid to ask questions. SAFETY
GOGGLES MUST BE WORN AT ALL TIMES. Students may NEVER work in a lab without
permission of the instructor or without supervision.
PREPARATION BEFORE THE LABORATORY
You will be able to work much more efficiently in the lab if you understand what it is you
are trying to do. READ THE TEXT BEFORE THE EXPERIMENT. Figure out how to prepare the
solutions before coming to lab so you don't waste valuable lab time. Be prepared. The time
spent in preparation is time that you won't have to spend in the lab.
1
